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Chemcial Industry and Engineering 2007, Vol. 24 Issue (6) :471-475    DOI:
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Preparation of Nanometer ZrO_2 with High Dispersibility by Microemulsion
JIA Chun-yao~(1,2),MA Zhi~1,WANG Yan-ji~2(1.School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China;2.School of Chemical Engineering,Heibei University of Technology,Tianjin 300130,China)
(1,2),MA Zhi~1,WANG Yan-ji~2(1.School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China;2.School of Chemical Engineering,Heibei University of Technology,Tianjin 300130,China

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Abstract Nanometer ZrO_2 with high dispersibility was prepared in microemulsion system of TX-10/n-hexanol/cyclohexane under the volume ratio of 1.0∶1.3∶7.7 with concentration of reactors for 0.02 mol/L,200 mL displacement dose of water and at the roasting temperature of 450 ℃.N_2 absorption experiments showed that there were corelations between pore size distribution and dispersibility of nanometer ZrO_2.XRD results revealed that the fresh sample was amorphous,and tetragonal phase appeared as a predominant phase with a little monoclinic modification after calcining the sample at 450 ℃ for 3 h.When further heating the sample at 750 ℃,pure monoclinic zirconia was obtained.
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Received 2007-11-15; published 2007-11-15
Cite this article:   
JIA Chun-yao~.Preparation of Nanometer ZrO_2 with High Dispersibility by Microemulsion[J]  Chemcial Industry and Engineering, 2007,V24(6): 471-475
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