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Chemcial Industry and Engineering 2009, Vol. 26 Issue (2) :99-102    DOI:
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Optimization for Synthesizing Anode Material of Li_4Ti_5O_(12)
MU Xue-mei,TANG Zhi-yuan(School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China)
(School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China

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Abstract Li_4Ti_5O_(12) was prepared by solid-state method with different sources of titanium(anatase,rutile,amorphous) and lithium(Li_2CO_3,LiOH·H_2O),the preparation of Li_4Ti_5O_(12) was optimized and Li_4Ti_5O_(12) was characterized.The experimental results showed that Li_4Ti_5O_(12) synthesized with anatase and Li_2CO_3 at 900 ℃ had better performance of lithium intercalation,excellent cyclicity,stable voltage,and higher first discharge capacity.In addition,during the process of Li~+ intercalation and de-intercalation,the crystal form of Li_4Ti_5O_(12) doesn't change.
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Received 2009-03-15; published 2009-03-15
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MU Xue-mei,TANG Zhi-yuan.Optimization for Synthesizing Anode Material of Li_4Ti_5O_(12)[J]  Chemcial Industry and Engineering, 2009,V26(2): 99-102
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