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Chemcial Industry and Engineering 1989, Vol. 6 Issue (4) :17-24    DOI:
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Crystallization Kinetics of Hexamethylenetetramine in a Vacuum Evaporation Crystallizer
Zhang You-Wen
(East China Institute of Chemical Technology) Qian Yu-Ying(Shanghai Research Invtitute of Chemical Engineering

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Abstract Hexamethylenetetramine crystallization kinetics is determined in a vacuum evaporation crystallizer with related Parameters. It is interesting to note that the crystallization of hexamethylenetetramine has special characteristics under Vacuum evaporation. The kinetics evaluated in this study is correlated by the equation: B°=39.94G1.1M_T-1.17 (TIPS) 1.68 It is shown that, for the system of hexamethylenetetramine with the index of crystal growth rate approximating to 1, the increase of the average crystal size of the product can not be obtained by simply increasing the crystal retention time. In order to obtain satisfactory size and size distributions of the product, it is very important to choose agitation speed because secondary nucleation is very much dependent on it.
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Received 1989-10-15; published 1989-10-15
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Zhang You-Wen .Crystallization Kinetics of Hexamethylenetetramine in a Vacuum Evaporation Crystallizer[J]  Chemcial Industry and Engineering, 1989,V6(4): 17-24
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