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Chemcial Industry and Engineering 2003, Vol. 20 Issue (6) :434-437    DOI:
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Synthesis and Characterization of Macromonomer Prepared by the Reaction of Polyether with Maleic Anhydride
L Shi-jun, GUO Rui-wei(School of Chemical Engineering,Tianjin University, Tianjin 300072, China)
(School of Chemical Engineering,Tianjin University, Tianjin 300072, China

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Abstract The structure of macromonomer (MM)synthesized by reacting polyether polyol with maleic anhydride(MA) was characterized with GPC,(()~1H)-NMR and double-bond titration.The results indicated that,besides the reaction of polyether with MA,the procedure also involved many chemical reactions including double-bond isomerization and double-bond addition.For double-bond addition,the molecular weight of MM increased,and the content of double-bond became less.Reaction temperature palyed an important role on the properities of MM which,including the content of double-bond,double-bond isomerization and molecular weight,resulted in the stability.At 120 ��,the stability of MM was best.
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Received 2003-11-15; published 2003-11-15
Cite this article:   
L Shi-jun, GUO Rui-wei.Synthesis and Characterization of Macromonomer Prepared by the Reaction of Polyether with Maleic Anhydride[J]  Chemcial Industry and Engineering, 2003,V20(6): 434-437
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