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Chemcial Industry and Engineering 2006, Vol. 23 Issue (1) :25-28    DOI:
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Clean Synthesis of 1,6-Dicarbamate Hexane
LU Ling,KANG Shi-fang,LI Guo-bing(School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China)
(School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China

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Abstract The clean synthesis of 1,6-dicarbamate hexane(HDC) from dimethyl carbonate(DMC) and 1,6-diamine hexane(HDA) is studied.The preparation of HDC using different catalysts is studied,and the activity of MgO/ZrO_2 is regarded better.After characterization of the catalyst,the activity of MgO in disperse phase is inferred higher than that of MgO in crystal phase.The quantitative analysis of HDC is carried out by HPLC analysis and the influence of different reaction conditions has been investigated.
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Received 2006-01-15; published 2006-01-15
Cite this article:   
LU Ling,KANG Shi-fang,LI Guo-bing.Clean Synthesis of 1,6-Dicarbamate Hexane[J]  Chemcial Industry and Engineering, 2006,V23(1): 25-28
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