LI Yong gang 1,LIU Dong zhi 1,QU Hong mei 1,MENG Dong yan 2 (1 School of Chemical Engineering,Tianjin University,Tianjin 300072,China; 2 Hengshui Normal Academy,Hebei Hengshui 053000,China)
(1 School of Chemical Engineering,Tianjin University,Tianjin 300072,China; 2 Hengshui Normal Academy,Hebei Hengshui 053000,China
Abstract The synthesis of N,N�� bis(trimethyl silyl)urea from trimethyl chlorosilane was mainly discussed.The reaction parameters including catalysts,temperature and molar ratio were optimized.Under the optimum condition,the yield of N,N�� bis(trimethylsilyl)urea was 57% on the basis of trimethyl chlorosilane.
LI Yong gang 1,LIU Dong zhi 1,QU Hong mei 1,MENG Dong yan 2 .Synthesis of N,N��-bis(trimethyl silyl)urea[J] Chemcial Industry and Engineering, 2000,V17(2): 0-0