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Chemcial Industry and Engineering 2003, Vol. 20 Issue (2) :67-70    DOI:
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Catalytic Synthesis of Piperonylene Propanal by KF/Al_2O_3
NA Ping1,HUANG Zong-liang1,LI Liang-long2,YU Yan-dong2emical Engineering and Technology,Tianjin University,Tianjin 300072,China;2.Perfumery.of.Jianzhong Chemicals,Sichuan Yibin 644000,China)

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Abstract Piperonylene propanal was synthesized through Claisen-Schmidt condensation reaction in the presence of KF/Al2O3,heliotropin and propanal as reactants.Adaptive technological conditions have been determined by statistical experiment.The yield of parallel experiment was 802% under the reaction conditions which are 60℃~70℃,03mol heliotropin and 042mol propanal as reactants,14g KF/Al2O3 catalyst,the dropping time of propanal 2h,reaction time 2h.
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Received 2003-03-15; published 2003-03-15
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NA Ping1,HUANG Zong-liang1,LI Liang-long2,YU Yan-dong2emical Engineering and Technology,Tianjin University,Tianjin 300072,China;2.Perfumery.of.Jianzhong Chemicals,Sichuan Yibin 644000,China).Catalytic Synthesis of Piperonylene Propanal by KF/Al_2O_3[J]  Chemcial Industry and Engineering, 2003,V20(2): 67-70
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