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Chemcial Industry and Engineering 2005, Vol. 22 Issue (2) :92-95    DOI:
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Synthesis of 1,2-O-isopropylidene-α-D-allofuranose
ZHANG Wei-hong,FENG Ya-qing,LIU Yun-hua,MENG Xiang-qi,LI Bin(School of Chemical Engineering,Tianjin University,Tianjin 300072,China)
(School of Chemical Engineering,Tianjin University,Tianjin 300072,China

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Abstract The synthesis of 1,2-O-diisopropylidene-α-D-allofuranose was studied in this paper. With α-D-glucose as raw material, 1,2-O-isopropylidene-α-D-allofuranose was synthesized by isopropylidenation and selective hydrolyzation. The main factors that influence the hydrolysis reaction were studied. The final product was characterized by (~1H-NMR),IR,TLC and other method. The overall yield is 45%. The route is simple and convenient.The raw material can be obtained easily. This method has great potential for application.
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Received 2005-03-15; published 2005-03-15
Cite this article:   
ZHANG Wei-hong,FENG Ya-qing,LIU Yun-hua,MENG Xiang-qi,LI Bin.Synthesis of 1,2-O-isopropylidene-α-D-allofuranose[J]  Chemcial Industry and Engineering, 2005,V22(2): 92-95
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