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Chemcial Industry and Engineering 2006, Vol. 23 Issue (4) :305-307    DOI:
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Synthesis of 3,3′,5,5′-Tetra-Tert Butylstilbene-4,4′-Quinone
XIA Dan,LI Xiang-gao,HOU Wei,WANG Shi-rong(School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China)
(School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China

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Abstract In this paper,3,3′,5,5′-tetra-tert-butylstilbene-4,4′-quinone is obtained from 2,6-ditertbutyl-p-methylphenol by the oxidation of potassium ferricyanide.The influences of the various conditions on the yield are studied. When the concentration of KOH is 5%(weight) and reaction time is 8 h,the highest yield of product is 40.34%.The composition and structure of product are determined by UV,IR,MS and elemental analysis.The HPLC purity is 99.79%.
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Received 2006-07-15; published 2006-07-15
Cite this article:   
XIA Dan,LI Xiang-gao,HOU Wei,WANG Shi-rong.Synthesis of 3,3′,5,5′-Tetra-Tert Butylstilbene-4,4′-Quinone[J]  Chemcial Industry and Engineering, 2006,V23(4): 305-307
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