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Chemcial Industry and Engineering 2007, Vol. 24 Issue (4) :367-369    DOI:
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Synthesis of N,N-diisopropylethylenediamine
DONG Yan-fei,QI Xin,ZHAO Wen-tao(School of Sciences,Tianjin University,Tianjin 300072,China)
(School of Sciences,Tianjin University,Tianjin 300072,China

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Abstract 2-amino ethyl hydrogen sulfate was prepared from aminoethanol and oil of vitriol and then was circlized by sodium hydroxide to get ethyleneimine.Ethyleneimine reacted with diisopropylamine in the presence of anhydrous aluminium chloride to obtain the target material of N,N-diisopropylethylenediamine.Structure of N,N-diisopropylethylenediamine was primarily identified by IR and()~1HNMR.
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Received 2007-07-15; published 2007-07-15
Cite this article:   
DONG Yan-fei,QI Xin,ZHAO Wen-tao.Synthesis of N,N-diisopropylethylenediamine[J]  Chemcial Industry and Engineering, 2007,V24(4): 367-369
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