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Chemcial Industry and Engineering 2008, Vol. 25 Issue (3) :203-207    DOI:
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Hydrolysis of Propyl Trimethoxy Silane
LI Fang-wen~(1,2),WU Jian-feng~2,XU Xiao-hong~2,WU Xiao-ai~1,MA Song-jiang~1(1.School of Chemistry and Chemical Engineering,Hunan University of Science and Technology,Xiangtan 411201,Hunan Province,China;2.School of Materials Science and Technology,Wuhan University of Technology,Wuhan 430070,Hubei Province,China)
(1,2),WU Jian-feng~2,XU Xiao-hong~2,WU Xiao-ai~1,MA Song-jiang~1(1.School of Chemistry and Chemical Engineering,Hunan University of Science and Technology,Xiangtan 411201,Hunan Province,China;2.School of Materials Science and Technology,Wuhan University of Technology,Wuhan 430070,Hubei Province,China

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Abstract In the paper,the hydrolysis of propyl trimethoxy silane(assigned with WD-10)was analyzed by the one-factor experimental method, conductivity detection and FTIR spectroscopy,and then the factors of affecting hydrolysis was discussed,the better technical parameters of hydrolysis were determined.The better technical parameters of hydrolysis are as follows: volumetric ratio of WD-10,secondary distilled water and methanol is 1∶1∶3;pH is 4;hydrolysis is at 30 ℃ for 4 h. This can provide reference for the oleophilic modification of porous ceramics filtering ball and the treatment of wastewater containing oil by coalescence filtration technique.
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Received 2008-05-15; published 2008-05-15
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LI Fang-wen~.Hydrolysis of Propyl Trimethoxy Silane[J]  Chemcial Industry and Engineering, 2008,V25(3): 203-207
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