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Chemcial Industry and Engineering 2010, Vol. 27 Issue (1) :17-20    DOI:
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Heterogeneous Esterification for the Synthesis of Butyl Acetate under the Condition of Microwave Irradiation
LIU Yan-xiu~1, LI Li-rong~1, ZHANG Tie-jing~2, ZHANG Wen-chao~3(1.Chemistry and Chemical Engineering College, Daqing Petroleum Institute, Daqing 163318, China;2.Daqing Chemical Plant 1, Daqing Petrochemical Company, Daqing 163714, China;3.Daqing Petrochemical Engineering Co. Ltd., Daqing 163714,China)
(1.Chemistry and Chemical Engineering College, Daqing Petroleum Institute, Daqing 163318, China;2.Daqing Chemical Plant 1, Daqing Petrochemical Company, Daqing 163714, China;3.Daqing Petrochemical Engineering Co. Ltd., Daqing 163714,China

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Abstract The synthesis of butyl acetate from acetic acid and n-butanol over HZSM-5 catalyst under the condition of microwave irradiation has been studied. The effects of amount of catalyst, microwave power, radiation time and amount of water absorbent were investigated. Under the suitable conditions, i.e., the volume ratio of acetic acid to n-butanol of 1.6, the amount of HZSM-5 of 0.094 g/mL (calculated based on acetic acid), the microwave irradiation power of 640 W, the microwave irradiation time of 30 min and the amount of calcium chloride of 0.375 g/mL (calculated based on acetic acid), the yield of butyl acetate could reach 98.7%.
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Received 2010-01-15; published 2010-01-15
Cite this article:   
LIU Yan-xiu~1, LI Li-rong~1, ZHANG Tie-jing~2, ZHANG Wen-chao~3.Heterogeneous Esterification for the Synthesis of Butyl Acetate under the Condition of Microwave Irradiation[J]  Chemcial Industry and Engineering, 2010,V27(1): 17-20
Copyright 2010 by Chemcial Industry and Engineering