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Chemcial Industry and Engineering 2013, Vol. 30 Issue (5) :52-54    DOI:
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IF5 Preparation Technics by GasSolid Reaction
 LIU  Chun-Xue, CUI  Xue-Wen, HAO  Shu-Hai

(Research Institute of Physical and Chemical Engineering of Nuclear Industry, Tianjin 300180, China)

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Abstract IF5 was prepared with I2 and F2 by gas-solid reaction, the flow rate of F2 is 28—30 L/min and reaction pressure is under -0.01 MPa. The influence of reaction temperature, molar ratio of reactants and adding amount of I2 were investigated. Results showed that the optimal conditions of preparing IF5 were: reaction temperature between 80—100 ℃, molar ratio of F2 to I2 is 6∶1, adding amount of I2 was 10 kg in 100 L reactor. Under these conditions,the biggest yield of IF5could reach 87.32% with purity of 99%.
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LIU Chun-Xue
CUI Xue-Wen
HAO Shu-Hai
KeywordsI2   F2   IF5    gas-solid reaction     
Received 2012-10-12;
Corresponding Authors: 刘春雪,电话:(022)84801504,E-mail:lcxhsss@163.com。      Email: lcxhsss@163.com
About author: 刘春雪(1980-),女,硕士,工程师,从事氟化物研究与开发。
Cite this article:   
LIU Chun-Xue, CUI Xue-Wen, HAO Shu-Hai.IF5 Preparation Technics by GasSolid Reaction[J]  Chemcial Industry and Engineering, 2013,V30(5): 52-54
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