Abstract The synthesis process of pmethylsulfonylphenylserine copper was studied in this paper.Methylsulfonylbenzaldehyde,glycine and copper sulfate were used as raw materials,and ammonia as catalyst.The results demonstrated the optimal conditions of the preparation process were as follows∶p-methylsulfonylbenzaldehyde∶glycine∶copper sulfate∶H2O=1∶11∶055∶170(molar ratio),reaction tempreture was 50 ℃,pH=9,reaction time was 30 hours.The yield of pmethylsulfonylphenylserine copper was approximately 80% under the optimal conditions.And they were characterized by TCL,LCMS and IR.The mechanism of the reaction was identified and the possible side reaction was speculated.
HAN Yu-Ying, SONG Jian, FENG Rong-Xiu, ZHAO Jun-Yan.Synthesis of p-Methylsulfonylphenylserine Copper[J] Chemcial Industry and Engineering, 2011,V28(2): 29-34
2011, Vol. 28 
