The Application Research of By-Products from the Manufacture of Piperazine
CHEN Li\|gong 1,WANG Jun\|bo 1,XU Zheng\|shuang 1,BAI Guo\|yi 1,LI Yang 1,MI Chang li 2 (1.School of Chemical Engineering,Tianjin University,Tianjin 300072,China; 2.Linyi City Scientific Commission of Shandong Province, Shangdong Linyi 276000,Ch
(1.School of Chemical Engineering,Tianjin University,Tianjin 300072,China; 2.Linyi City Scientific Commission of Shandong Province, Shangdong Linyi 276000,C
Abstract:
The application of the by\|products(mixture of N\|hydroxyethyl\|piperazine and N\|β\|hydroxyethyl\|ethylenediamine)from the manufacture of piperazine was involved in this paper.Using Ba\|Sr\|2 as catalyst and the mixture of N\|hydroxyethyl\|piperizine and N\|β hydroxyethyl ethylenediamine as the materials to synthesize triethylenediamine,the result showed when operating at a temperature range of 360℃ and 380℃,the yield of triethylenediamine was over 60% and the purity was 99.9%.
CHEN Li\|gong 1,WANG Jun\|bo 1,XU Zheng\|shuang 1,BAI Guo\|yi 1,LI Yang 1,MI Chang li 2 .The Application Research of By-Products from the Manufacture of Piperazine[J]. Chemcial Industry and Engineering, 2000,17(6): 341-345