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��ѧ��ҵ�빤�� 2005, Vol. 22 Issue (6) :427-429    DOI:
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Synthesis of N-phenyl Maleimide by Decompressed Azeotropic Method
WANG Dong-hui,FENG Ya-qing,LIANG Zu-pei,SHI Da-xin(School of Chemical Engineering,Tianjin University,Tianjin 300072,China)
(School of Chemical Engineering,Tianjin University,Tianjin 300072,China

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Abstract�� N-phenyl maleimide was synthesized from maleic anhydride and aniline.Decompressed azeotropic method,a totally new method for the preparation of N-phenyl maleimide(N-PMI),is developed on the basis of acetic anhydride method and atmospheric azeotropic method.The reaction is carried out in the presence of orthophosphoric acid,with the yield of NPMI above 85%,and the purity of product above 95%.
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Received 2005-11-15; published 2005-11-15
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������,������,������,ʷ���.��ѹ���з��ϳ�N-�����������ǰ�[J].  ��ѧ��ҵ�빤��, 2005,22(6): 427-429
WANG Dong-hui,FENG Ya-qing,LIANG Zu-pei,SHI Da-xin.Synthesis of N-phenyl Maleimide by Decompressed Azeotropic Method[J].  Chemcial Industry and Engineering, 2005,22(6): 427-429
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