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化学工业与工程
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��ѧ��ҵ�빤�� 2008, Vol. 25 Issue (3) :271-272    DOI:
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Preparing 2-Fluoring-5-Nitroaniline by Reduction of Zinc Powder
WANG Qian,QIN Hai-fang(Changzhou Institute of Engineering Technology,Changzhou 213164,Jiangsu Province,China)
(Changzhou Institute of Engineering Technology,Changzhou 213164,Jiangsu Province,China

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Abstract�� In this paper,2-fluorin-5-nitroaniline was prepared by reduction of 2,4-dinitrofluorin benzene catalyzed by zinc powder in the mixed solvent of ethanol/water.The optimum conditions were as follows: when mol ratio of 2,4-dinitrofluorin benzene to zinc power was 1��4,mol ratio of ethanol to water in the mixed solvent was 3��2 under refluxing at 50��(60 ��),the yield reached 70.1%.
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Received 2008-05-15; published 2008-05-15
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��Ǭ;�غ���;.п�ۻ�ԭ���Ʊ�2-��-5-��������[J].  ��ѧ��ҵ�빤��, 2008,25(3): 271-272
WANG Qian,QIN Hai-fang.Preparing 2-Fluoring-5-Nitroaniline by Reduction of Zinc Powder[J].  Chemcial Industry and Engineering, 2008,25(3): 271-272
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